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Menghao SHEN, Bo LIU, Yuehui QIAO, et al. Analysis of Key Acidic Aroma Components of Canadian Tobacco Leaves Mainstream Smoke Based on Odor Activity Value[J]. JOURNAL OF YUNNAN AGRICULTURAL UNIVERSITY(Natural Science), 2023, 38(3): 456-464. DOI: 10.12101/j.issn.1004-390X(n).202209057
Citation: Menghao SHEN, Bo LIU, Yuehui QIAO, et al. Analysis of Key Acidic Aroma Components of Canadian Tobacco Leaves Mainstream Smoke Based on Odor Activity Value[J]. JOURNAL OF YUNNAN AGRICULTURAL UNIVERSITY(Natural Science), 2023, 38(3): 456-464. DOI: 10.12101/j.issn.1004-390X(n).202209057

Analysis of Key Acidic Aroma Components of Canadian Tobacco Leaves Mainstream Smoke Based on Odor Activity Value

More Information
  • Received Date: September 26, 2022
  • Revised Date: May 09, 2023
  • Accepted Date: May 09, 2023
  • Available Online: May 14, 2023
  • Published Date: May 29, 2023
  • Purpose To identify the key acidic aroma components in Canadian tobacco leaves mainstream smoke, providing a reference for the development of flavor with Canadian tobacco style characteristics.
    Methods Using the acidic components of mainstream smoke of Canadian tobacco leaves as the research object, the reasonable and effective segmentation was carried out through column chromatography and medium pressing preparation technology. Guided by sensory evaluation and combined with GC-MS analysis, the characteristic groups were determined. The important acidic aroma components were quantitatively analyzed and the corresponding odor activity value (odor activity value, OAV) was calculated.
    Results 1) The acidic characteristic components of Canadian tobacco leaves smoke were mainly small molecule acid and aromatic acid groups, and 16 important acidic aroma components of them were identified. The mass concentration of isovaleric acid (1.09 mg/mL) and phenylacetic acid (6.44 mg/mL) were the highest in small molecular acid and aromatic acid group, respectively. 2) The OAV of 16 components were all greater than one, among which isovaleric acid and phenylacetic acid had the largest OAV.
    Conclusion Isovaleric acid and phenylacetic acid are the key acidic aroma components in mainstream smoke of Canadian tobacco leaves.
  • [1]
    赖燕华, 汪军霞. 有机酸对卷烟感官风格和品质的影响研究[J]. 分析测试学报, 2015, 34(6): 696. DOI: 10.3969/j.issn.1004-4957.2015.06.012.
    [2]
    张迎春, 郭国宁, 岳海波, 等. 卷烟主流烟气气相物和总粒相物中有机酸的分析研究[J]. 分析科学学报, 2010, 26(5): 567.
    [3]
    张启东, 刘俊辉, 张文娟, 等. 初烤烟叶提取物中关键甜味成分的感官导向分析[J]. 烟草科技, 2016, 49(6): 58. DOI: 10.16135/j.issn1002-0861.20160609.
    [4]
    米冠杰, 顾文博, 孙文梁, 等. 卷烟烟气重要酸性香味成分的分离制备与鉴定[J]. 烟草科技, 2013(10): 49. DOI: 10.3969/j.issn.1002-0861.2013.10.012.
    [5]
    贾春晓, 张月丽, 陈芝飞, 等. 卷烟烟气中性香味成分的半制备HPLC分离与GC-MS测定[J]. 轻工学报, 2017, 32(6): 63. DOI: 10.3969/j.issn.2096-1553.2017.6.008.
    [6]
    宋焕禄. 分子感官科学[M]. 北京: 科学出版社, 2014.
    [7]
    陈芝飞, 蔡莉莉, 郝辉, 等. 香气活力值在食品关键香气成分表征中的应用研究进展[J]. 食品科学, 2018, 39(19): 329. DOI: 10.7506/spkx1002-6630-201819049.
    [8]
    冒德寿, 李智宇, 刘强, 等. 基于味觉活力值的烤烟主流烟气关键酸味物质的研究[J]. 中国烟草学报, 2014, 20(6): 21. DOI: 10.3969/j.issn.1004-5708.2014.06.004.
    [9]
    迟广俊, 刘俊辉, 鲍峰, 等. 初烤烟叶提取物中酸味关键成分的感官导向分析[J]. 烟草科技, 2015, 48(12): 27. DOI: 10.16135/j.issn1002-0861.20151205.
    [10]
    张启东, 刘俊辉, 柴国璧, 等. 主流烟气粒相物水溶性组分中烤甜香成分分析[J]. 烟草科技, 2014(6): 54. DOI: 10.3969/j.issn.1002-0861.2014.06.012.
    [11]
    史清照, 柴国璧, 汪军霞, 等. 卷烟主流烟气粒相物酸味成分感官导向分析[J]. 烟草科技, 2019, 52(11): 30. DOI: 10.16135/j.issn1002-0861.2019.0294.
    [12]
    陈芝飞, 杨靖, 马宇平, 等. 基于活性阈值的卷烟烟气中重要碱性香气成分剖析[J]. 烟草科技, 2017, 50(3): 39. DOI: 10.16135/j.issn1002-0861.2016.0408.
    [13]
    CHEN Z F, YANG J, SUN Z T, et al. Determination of odor activity values (OAVs) of selected volatile organic acids in mainstream cigarette smoke[J]. Tobacco Science & Technology, 2016, 49(S1): 27. DOI: 10.16135/j.issn1002-0861.2016.0404.
    [14]
    杨靖, 宋梦坤, 杨鹏飞, 等. 基于香气活力值的烤烟烟叶清(青)香风格特征分析[J]. 烟草科技, 2020, 53(1): 34. DOI: 10.16135/j.issn1002-0861.2019.0132.
    [15]
    范武, 张启东, 刘俊辉, 等. 卷烟主流烟气酸香特征成分组群的分布特征及感官贡献[J]. 烟草科技, 2020, 53(1): 65. DOI: 10.16135/j.issn1002-0861.2019.0379.
    [16]
    胡安福, 范武, 夏倩, 等. 卷烟主流烟气焦甜、奶香和豆香特征成分组群的分布特征和感官贡献[J]. 烟草科技, 2020, 53(12): 27. DOI: 10.16135/j.issn1002-0861.2020.0203.
    [17]
    朱浩, 柴国璧, 迟广俊, 等. 卷烟主流烟气烟熏香成分的感官导向分析[J]. 烟草科技, 2017, 50(1): 41. DOI: 10.16135/j.issn1002-0861.2016.0431.
    [18]
    茅中一, 洪祖灿, 刘加增, 等. 基于香气活性值的福建尤溪烟叶提取物香气特征成分分析[J]. 烟草科技, 2020, 53(10): 56. DOI: 10.16135/j.issn1002-0861.2020.0233.
    [19]
    杨鹏飞, 张增辉, 何春雨, 等. 基于分子感官科学的烟用香精关键香气活性成分分析[J]. 轻工学报, 2021, 36(2): 34. DOI: 10.12187/2021.02.005.
    [20]
    蒋薇, 司晓喜, 张凤梅, 等. 酸类香料在不同加香方式制备卷烟中的感官贡献度研究[J]. 轻工学报, 2022, 37(1): 95. DOI: 10.12187/2022.01.013.
    [21]
    杨靖, 毛多斌, 陈芝飞, 等. GC-MS/O技术测定卷烟烟气中巨豆三烯酮的香气活力值[J]. 中国烟草学报, 2016, 22(6): 11. DOI: 10.16472/j.chinatobacco.2015.491.
    [22]
    KRÜSEMANN E J Z, CREMERS J W J M, VISSER W F, et al. The sensory difference threshold of menthol odor in flavored tobacco determined by combining sensory and chemical analysis[J]. Chemical Senses, 2017, 42(3): 233. DOI: 10.1093/chemse/bjw123.
    [23]
    GB/T 19609—2004. 卷烟 用常规分析用吸烟机测定总粒相物和焦油[S].
    [24]
    洪华俏. 卷烟主流烟气中香气成分的研究[D]. 长沙: 湖南农业大学, 2008.
    [25]
    YC/T 497—2014. 卷烟 中式卷烟风格感官评价方法[S].
    [26]
    谢剑平. 烟草香原料[M]. 北京: 化学工业出版社, 2009.
    [27]
    孙宝国, 刘玉平. 食用香料手册[M]. 北京: 中国石化出版社, 2004.
    [28]
    LEFFINGWELL J C, YIUNG H J, BERNASEK E. Tobacco flavoring for smoking products[M]. North Carolina: Reynolds Tobacco Company, 1972.
    [29]
    VAN GEMERT L J. Odour thresholds: compilation of odour threshold values in air, water and other media[M]. Utrecht: Oliemans Punter & Partners BV, 2011.
    [30]
    FÉCHIR M, REGLITZ K, MALL V, et al. Molecular insights into the contribution of specialty barley malts to the aroma of bottom-fermented lager beers[J]. Journal of Agricultural and Food Chemistry, 2021, 69(29): 8190. DOI: 10.1021/acs.jafc.1c01846.
    [31]
    ONG P, ACREE T E, LAVIN E H. Characterization of volatiles in rambutan fruit (Nephelium lappaceum L.)[J]. Journal of Agricultural and Food Chemistry, 1998, 46(2): 611. DOI: 10.1021/jf970665t.
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